FORMATION OF THE DINITRO-3H-PYRAZOLE DERIVATIVE  OF CYCLOARTEMISIAKETONE OXIME

Suleimenov, E. M.; Atazhanova, G. A.; Kulyyasov, A. T.; Raldugin, V. A.; Bagryanskaya, I. Yu.; Gatilov, Yu. V.; Shakirov, M. M.; Adekenov, S. M.

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FORMATION OF THE DINITRO-3H-PYRAZOLE DERIVATIVE OF CYCLOARTEMISIAKETONE OXIME

Suleimenov, E. M.; Atazhanova, G. A.; Kulyyasov, A. T.; Raldugin, V. A.; Bagryanskaya, I. Yu.; Gatilov, Yu. V.; Shakirov, M. M.; Adekenov, S. M.

URI: http://dspace.enu.kz/handle/data/11764

Date: 2014-07-02

Abstract:

(3aR*,6aR*)-3,3,5,5-Tetramethyl-3a,6a-dinitro-3a,6a-dihydro-3H-cyclopentano[c]pyrazol-2-oxide was formed by reaction of cycloartemisiaketone oxime [4,4-dimethyl-2-(1-methylethylidene)cyclopentanone oxime] with AcOH and NaNO2 in CHCl3 solution. The structure was solved by x-ray structure analysis.